{"id":2259,"date":"2023-03-31T08:57:38","date_gmt":"2023-03-31T08:57:38","guid":{"rendered":"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=2259"},"modified":"2023-03-31T08:57:38","modified_gmt":"2023-03-31T08:57:38","slug":"discussion-the-masters-thesis-synthesis-characterization-and-antimicrobial-activity-evaluation-of-new-3-acetylcoumarin-chalcone-conjugate-derivatives","status":"publish","type":"post","link":"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=2259","title":{"rendered":"Discussion the Master&#8217;s Thesis \u201cSynthesis, Characterization and Antimicrobial Activity Evaluation of New 3-Acetylcoumarin \u2013 Chalcone Conjugate Derivatives"},"content":{"rendered":"<div class=\"wpb-content-wrapper\"><p>[vc_row][vc_column][vc_column_text]<\/p>\n<p style=\"text-align: justify;\"><span style=\"font-size: 19px;\">The Faculty of Pharmacy discussed the Master thesis \u201c<strong>Synthesis,Characterization and Antimicrobial Activity Evaluation of New 3-Acetylcoumarin \u2013 Chalcone Conjugate Derivatives)<\/strong>\u201d by the master student <strong>Tuka Hassan Abd-Elhussain<\/strong> and the supervisor: <strong>Dr. Muthanna S. Farhan<\/strong> in the <strong>pharmaceutical chemistry<\/strong> Department.\u00a0The study aimed to synthesize a new series of pyrazoline and pyrimidine derivatives and examine their ability to inhibit the growth of microorganisms as part of an effort to generate new compounds that exhibit enhanced antimicrobial activity. In order to synthesize new bioactive pharmacophores, 3-acetyl coumarin-chalcone hybrids (2a-c) were utilized as flexible precursors in the synthesis process. In this particular investigation, salicylaldehyde and ethyl acetoacetate interacted to produce 3-acetyl coumarin (compound 1). Condensation of 3- acetylcoumarin with aromatic aldehydes in the presence of piperidine as a catalyst was used to produce 3-acetyl coumarin-chalcone hybrids (compounds 2a-c). In order to produce pyrazoline derivatives, these intermediates reacted under reflux with hydrazine hydrate in the presence of glacial acetic acid as a catalyst to form pyrazoline derivatives (compounds 3a-c) and with semicarbazide and NaOH ,serving as the catalytic agents, to form substituted pyrazoline derivatives (compounds 4a-c) . pyrimidine derivatives ( compounds 5a-c) were produced by reacting these hybrids under reflux with thoiurea in the presence of NaOH as a catalyst in ethanol. The FT-IR and 1HNMR spectroscopy were used to conduct an analysis on the pyrimidine and pyrazoline derivatives that were successfully synthesized as the final target compounds. Antimicrobial activity of the synthesized compounds was tested on two gram-positive bacteria (S. aureus and S. pyogenes), two gram-negative bacteria (E. coli, p. aeruginosa), and one fungal species (C. ablicans). Compounds 4b and 4c exhibited the greatest antibacterial activity against both gram-positive and gram-negative bacteria. Compounds 3a, 4b, 5a, 5b, and 5c had the most potent inhibitory effects against C. ablicans.<\/span><\/p>\n<p>[\/vc_column_text][\/vc_column][\/vc_row][vc_row][vc_column]<div id=\"cz_20194\" class=\"cz_grid_p cz_20194\"><div class=\"cz_grid cz_grid_1 clr cz_grid_c4 cz_grid_1_no_title cz_grid_1_mid tac cz_tooltip cz_grid_1_no_title\"><div class=\"cz_grid_item cz_grid_first\"><\/div><div class=\"cz_grid_item \"><div data-title=\"viber_image_2023-03-31_07-30-18-802\"><a class=\"cz_grid_link \" href=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/03\/viber_image_2023-03-31_07-30-18-802.jpg\" data-xtra-lightbox><img loading=\"lazy\" decoding=\"async\" width=\"600\" height=\"600\" src=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/03\/viber_image_2023-03-31_07-30-18-802-600x600.jpg\" class=\"attachment-codevz_600_600\" alt=\"\" title=\"viber_image_2023-03-31_07-30-18-802\" srcset=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/03\/viber_image_2023-03-31_07-30-18-802-600x600.jpg 600w, https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/03\/viber_image_2023-03-31_07-30-18-802-150x150.jpg 150w\" sizes=\"auto, (max-width: 600px) 100vw, 600px\" \/><div class=\"cz_grid_details\"><i class=\"fa fa-search cz_grid_icon\"><\/i><\/div><\/a><\/div><\/div><\/div><\/div>[\/vc_column][\/vc_row]<\/p>\n<\/div>","protected":false},"excerpt":{"rendered":"<p>[vc_row][vc_column][vc_column_text] The Faculty of Pharmacy discussed the Master thesis \u201cSynthesis,Characterization and Antimicrobial Activity Evaluation of New 3-Acetylcoumarin \u2013 Chalcone Conjugate &#8230; <a class=\"cz_readmore\" href=\"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=2259\"><i class=\"fa czico-132-arrows-8\" aria-hidden=\"true\"><\/i><span>more<\/span><\/a><\/p>\n","protected":false},"author":9,"featured_media":2260,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"","_lmt_disable":"","footnotes":""},"categories":[3,7],"tags":[],"class_list":["post-2259","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-latest-news","category-dissuasion"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.8 - 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