{"id":3923,"date":"2023-10-01T19:28:04","date_gmt":"2023-10-01T19:28:04","guid":{"rendered":"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=3923"},"modified":"2023-10-01T19:28:04","modified_gmt":"2023-10-01T19:28:04","slug":"discussion-the-synthesis-characterization-and-preliminary-antimicrobial-activity-evaluation-of-mannich-base-derivatives-of-isatin-and-5-fluoroisatin-schiff-base-conjugates","status":"publish","type":"post","link":"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=3923","title":{"rendered":"Discussion \u00a0the Synthesis, Characterization, and Preliminary Antimicrobial Activity Evaluation of Mannich Base Derivatives of Isatin and 5-Fluoroisatin Schiff Base Conjugates"},"content":{"rendered":"<div class=\"wpb-content-wrapper\"><p>[vc_row][vc_column][vc_column_text]<\/p>\n<p style=\"text-align: justify;\"><span style=\"font-size: 19px;\">The College of Pharmacy discussed the master\u2019s thesis entitled Synthesis, Diagnosis, and Evaluation of the Primary Biological Activity of Mannich Base Derivatives from Isatin and 5-Fluoroisatin, Schiff Base Derivatives, by the student <strong>Mustafa Mahmoud Mukhlif<\/strong> and his supervisor, Assistant Professor <strong>May Muhammad Jawad Al-Mudhafar <\/strong>in the Pharmaceutical Chemistry Department.\u00a0The thesis <strong>aimed<\/strong> to synthesize twelve different compounds of isatin and 5-fluoroisatin by linking them to different secondary amines in the Mannich reaction to obtain the intermediate compounds, which enter the second step of the reaction by linking them to phenylhydrazine in a Schiff base reaction to obtain the final compounds as follows:\u00a0The first step is to prepare twelve different intermediate compounds by condensing the secondary amines with isatin and 5-fluoroisatin using formalin at a concentration of 37%, where tetrahydrofuran is used as a solvent.\u00a0The second step is to prepare the final compounds, using the compounds resulting from the first step and their reactant, phenylhydrazine, using a condenser in the presence of glacial acetic acid as a catalyst for the reaction and absolute ethanol as a solvent.\u00a0The actives were monitored using thin-layer chromatography to ensure the completion of the reactions and the purity of the resulting compounds.\u00a0The final compounds were examined using the melting point of the compound, infrared spectroscopy, and proton nuclear magnetic resonance spectroscopy, and the results showed good agreement with the compounds that were prepared.\u00a0An evaluation of the biological effectiveness of the final prepared compounds was conducted against two types of gram-positive bacteria and four types of gram-negative bacteria, and the results showed good effectiveness of the compounds compared to the standard compounds (amoxicillin and ciprofloxacin).The biological effectiveness of one type of fungus was also evaluated, and the <strong>results<\/strong> showed strong effectiveness compared to the standard compound flucon<\/span><\/p>\n<p>[\/vc_column_text][\/vc_column][\/vc_row][vc_row][vc_column]<div id=\"cz_80847\" data-position=\"top-right\" class=\"cz_80847 cz_image clr cz_image_no_fx center_on_mobile\"><div class=\"\" ><div class=\"cz_image_in\"><div class=\"cz_main_image\"><img loading=\"lazy\" decoding=\"async\" width=\"1600\" height=\"1066\" src=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1.jpg\" class=\"attachment-full\" alt=\"\" title=\"1\" srcset=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1.jpg 1600w, https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1-300x200.jpg 300w, https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1-1024x682.jpg 1024w, https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1-768x512.jpg 768w, https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1-1536x1023.jpg 1536w, https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/10\/1-600x400.jpg 600w\" sizes=\"auto, (max-width: 1600px) 100vw, 1600px\" \/><\/div><\/div><\/div><\/div>[\/vc_column][\/vc_row]<\/p>\n<\/div>","protected":false},"excerpt":{"rendered":"<p>[vc_row][vc_column][vc_column_text] The College of Pharmacy discussed the master\u2019s thesis entitled Synthesis, Diagnosis, and Evaluation of the Primary Biological Activity of &#8230; <a class=\"cz_readmore\" href=\"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=3923\"><i class=\"fa czico-132-arrows-8\" aria-hidden=\"true\"><\/i><span>more<\/span><\/a><\/p>\n","protected":false},"author":9,"featured_media":3924,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"","_lmt_disable":"","footnotes":""},"categories":[3,7],"tags":[],"class_list":["post-3923","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-latest-news","category-dissuasion"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.8 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Discussion \u00a0the Synthesis, Characterization, and Preliminary Antimicrobial Activity Evaluation of Mannich Base Derivatives of Isatin and 5-Fluoroisatin Schiff Base Conjugates - College of Pharmacy<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" 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