{"id":4644,"date":"2023-12-18T19:03:58","date_gmt":"2023-12-18T19:03:58","guid":{"rendered":"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=4644"},"modified":"2023-12-18T19:03:58","modified_gmt":"2023-12-18T19:03:58","slug":"the-faculty-of-pharmacy-discussed-the-synthesis-and-characterization-of-new-acetohydrazide-derivatives-as-possible-antimicrobial-agents","status":"publish","type":"post","link":"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=4644","title":{"rendered":"The Faculty of Pharmacy Discussed the Synthesis and Characterization of New Acetohydrazide Derivatives as Possible Antimicrobial Agents"},"content":{"rendered":"<div class=\"wpb-content-wrapper\"><p>[vc_row][vc_column][vc_column_text]<\/p>\n<p style=\"text-align: justify;\"><span style=\"font-size: 19px;\">The Faculty of Pharmacy discussed the MSc thesis entitled \u201cSynthesis and Characterization of New 2-(2-Oxo-2H-Chromen-4-yl) Acetohydrazide Derivatives as Possible Antimicrobial Agents&#8221; by Kaarrar Ahmed Hachim and his supervisor, Assistant Professor Dr. Mohammed Kamil Hadi in the Pharmaceutical Chemistry Department.\u00a0The study aimed to synthesize compound III, 2-[(2-oxo-2H-chromen-4-yl)oxy]acetohydrazide, starting from compound I, 4-hydroxycoumarin. Two new series of 2-[(2-oxo-2H-chromen-4-yl)oxy] acetohydrazides (compound III) have been synthesized with the aim of investigating their use as antimicrobial agents.\u00a0The study included the synthesis of the first series, N-alkyl hydrazide (IV a-c), by the reaction of compound III with different halides in the presence of triethylamine (TEA) and N,N-dimethylformamide (DMF). The second series, N-acyl hydrazones (Schiff bases) (V a\u2013d), was made by reacting compound III with various aldehydes in the presence of ethanol and glacial acetic acid. The target compounds were synthesized successfully, and their structures were characterized using ATR-FTIR and HNMR spectrum spectroscopy.\u00a0All the new derivatives (IV a-c, V a-d) were studied for their in-vitro antimicrobial activity using the well diffusion technique. Utilizing amoxicillin and ciprofloxacin as standard antibacterial agents, antibacterial activity was tested against four different types of bacteria: two Gram-positive (G+ve) bacteria (<em>Streptococcus pneumoniae <\/em>and <em>Staphylococcus aureus<\/em>) and two Gram-negative (G-ve) bacteria (<em>Escherichia coli<\/em> and <em>Pseudomonas aeruginosa<\/em>). Antifungal activity was tested against <em>Candida albicans<\/em> using fluconazole as a standard antifungal agent.\u00a0The results showed that all derivatives IV (a-c) and V (a-d) showed high antibacterial efficacy against Gram-positive and Gram-negative bacteria. All the investigated compounds showed notable effectiveness against <em>Candida albicans <\/em>compared to fluconazole, except compound IVa, which showed moderate activity.<\/span><\/p>\n<p>[\/vc_column_text][\/vc_column][\/vc_row][vc_row][vc_column]<div id=\"cz_109055\" class=\"cz_grid_p cz_109055\"><div class=\"cz_grid cz_grid_1 clr cz_grid_c1 cz_grid_l1 cz_grid_1_no_title cz_grid_1_mid tac cz_tooltip cz_grid_1_no_title\"><div class=\"cz_grid_item cz_grid_first\"><\/div><div class=\"cz_grid_item \"><div data-title=\"1\"><a class=\"cz_grid_link \" href=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/12\/1-16.jpg\" data-xtra-lightbox><img loading=\"lazy\" decoding=\"async\" width=\"1192\" height=\"500\" src=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/12\/1-16-1192x500.jpg\" class=\"attachment-codevz_1200_500\" alt=\"\" title=\"1\" \/><div class=\"cz_grid_details\"><i class=\"fa fa-search cz_grid_icon\"><\/i><\/div><\/a><\/div><\/div><div class=\"cz_grid_item \"><div data-title=\"2\"><a class=\"cz_grid_link \" href=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/12\/2-11.jpg\" data-xtra-lightbox><img loading=\"lazy\" decoding=\"async\" width=\"959\" height=\"500\" src=\"https:\/\/en.copharm.uobaghdad.edu.iq\/wp-content\/uploads\/sites\/80\/2023\/12\/2-11-959x500.jpg\" class=\"attachment-codevz_1200_500\" alt=\"\" title=\"2\" \/><div class=\"cz_grid_details\"><i class=\"fa fa-search cz_grid_icon\"><\/i><\/div><\/a><\/div><\/div><\/div><\/div>[\/vc_column][\/vc_row]<\/p>\n<\/div>","protected":false},"excerpt":{"rendered":"<p>[vc_row][vc_column][vc_column_text] The Faculty of Pharmacy discussed the MSc thesis entitled \u201cSynthesis and Characterization of New 2-(2-Oxo-2H-Chromen-4-yl) Acetohydrazide Derivatives as Possible &#8230; <a class=\"cz_readmore\" href=\"https:\/\/en.copharm.uobaghdad.edu.iq\/?p=4644\"><i class=\"fa czico-132-arrows-8\" aria-hidden=\"true\"><\/i><span>more<\/span><\/a><\/p>\n","protected":false},"author":9,"featured_media":4645,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_lmt_disableupdate":"","_lmt_disable":"","footnotes":""},"categories":[3,7],"tags":[],"class_list":["post-4644","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-latest-news","category-dissuasion"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.8 - 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